发明名称 |
PROCESS FOR PREPARING DIGLYCERINE |
摘要 |
PCT No. PCT/EP94/00834 Sec. 371 Date Sep. 25, 1995 Sec. 102(e) Date Sep. 25, 1995 PCT Filed Mar. 16, 1994 PCT Pub. No. WO94/21582 PCT Pub. Date Sep. 29, 1994A process for preparing diglycerol in high concentrations and high yields by partially reacting glycerol in the presence of an alkaline catalyst to form a reaction mixture containing from 10 to 15% by weight of diglycerol and separating the unreacted glycerol from the reaction mixture in a wiped film or short path first distillation zone at a reduced pressure of 0.5 to 5 mbar and distilling a bottoms product from the first distillation zone in a second distillation zone which is a short path distillation zone at a pressure of 0.05 to 0.3 mbar to obtain a second bottom product containing at least 90% by weight diglycerol. Diglycerol of higher purity can be obtained by recovering diglycerol as a distillate from a third distillation zone. |
申请公布号 |
EP0693050(B1) |
申请公布日期 |
1997.10.01 |
申请号 |
EP19940911183 |
申请日期 |
1994.03.16 |
申请人 |
HENKEL KOMMANDITGESELLSCHAFT AUF AKTIEN |
发明人 |
JEROMIN, LUTZ;GUTSCHE, BERNHARD;BUNTE, REINHARD;JORDAN, VOLKMAR |
分类号 |
B01J23/02;C07C41/09;C07C41/42;C07C43/13;(IPC1-7):C07C43/13 |
主分类号 |
B01J23/02 |
代理机构 |
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代理人 |
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主权项 |
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地址 |
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