发明名称 Preparation of a pure dialkylaminoethanol stable against discoloration
摘要 A process for the preparation of a color-stable dialkylaminoethanol of the formula <IMAGE> in which R1 and R2 independently are C1-C20-alkyl, by reacting ethylene oxide with a dialkylamine of the formula HNR1R2, in which R1 and R2 have the same meaning, in the presence of from 2.5 to 50% by weight of water, based on the reaction mixture, at a temperature of from 95 DEG to 170 DEG C., and separating off the water and high-boiling constituents by distillation under a reduced pressure and at a temperature of from 40 DEG to 90 DEG C. at the column bottom.
申请公布号 US5663444(A) 申请公布日期 1997.09.02
申请号 US19950497072 申请日期 1995.06.30
申请人 BASF AKTIENGESELLSCHAFT 发明人 MELDER, JOHANN-PETER;RUIDER, GUENTHER;WITZEL, TOM;ROSS, KARL-HEINZ;BOETTGER, GUENTER
分类号 C07C213/04;C07C213/10;C07C215/08;(IPC1-7):C07C209/02 主分类号 C07C213/04
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