发明名称 |
Preparation of a pure dialkylaminoethanol stable against discoloration |
摘要 |
A process for the preparation of a color-stable dialkylaminoethanol of the formula <IMAGE> in which R1 and R2 independently are C1-C20-alkyl, by reacting ethylene oxide with a dialkylamine of the formula HNR1R2, in which R1 and R2 have the same meaning, in the presence of from 2.5 to 50% by weight of water, based on the reaction mixture, at a temperature of from 95 DEG to 170 DEG C., and separating off the water and high-boiling constituents by distillation under a reduced pressure and at a temperature of from 40 DEG to 90 DEG C. at the column bottom.
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申请公布号 |
US5663444(A) |
申请公布日期 |
1997.09.02 |
申请号 |
US19950497072 |
申请日期 |
1995.06.30 |
申请人 |
BASF AKTIENGESELLSCHAFT |
发明人 |
MELDER, JOHANN-PETER;RUIDER, GUENTHER;WITZEL, TOM;ROSS, KARL-HEINZ;BOETTGER, GUENTER |
分类号 |
C07C213/04;C07C213/10;C07C215/08;(IPC1-7):C07C209/02 |
主分类号 |
C07C213/04 |
代理机构 |
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代理人 |
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主权项 |
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地址 |
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