发明名称 |
Process for preparing protocatechualdehyde |
摘要 |
<p>Protocatechualdehyde is prepared by the steps of reacting piperonyl dichloride with molecular chlorine in the presence of phosphorus trichloride, phosphorus pentachloride or sulfuryl chloride to prepare dichloropiperonylidene dichloride and hydrolyzing the dichloropiperonylidene dichloride. The piperonyl dichloride can be prepared by the reaction of piperonal with thionyl chloride in the presence of dimethylformamide.</p> |
申请公布号 |
EP0786446(A1) |
申请公布日期 |
1997.07.30 |
申请号 |
EP19970101046 |
申请日期 |
1997.01.23 |
申请人 |
UBE INDUSTRIES, LTD. |
发明人 |
HARADA, KATSUMASA;SHIRAI, MASASHI;FURUYA, TOSHIO;KURODA, NOBUYUKI |
分类号 |
C07C45/43;C07D317/46;(IPC1-7):C07C45/43;C07C47/565 |
主分类号 |
C07C45/43 |
代理机构 |
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代理人 |
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主权项 |
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地址 |
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