发明名称 PROCESS FOR THE PRODUCTION OF UNHYDROUS ETHYLEN CHLORHYDRIN WITH HIGH PURITY
摘要 To the reactor of the first stage (R01) with ethylenechlorohydrine is through the mixer (Z01) under continuous circulation of the reactive shaft added dry salt acid, later through the mixer (Z02) ethylene oxide. The reactive heat is removed by the heat exchanger (E01). Concurrently with the salt acid saturation washing the gases begins in the absorber over (R01) by undercooled raw ethylenechlorohydrine from the reactor of the second stage (R02) and to the (R02) is added ethylene oxide through the mixer (Z03). Degas from (R02) is conducted to the bottom part of the second absorber, countercurrently is sprinkled by the raw ethylenechlorohydrine, saturated salt acid, outgoing overflow from (R01). The raw ethylenechlorohydrine is continuously conducted to the reservoir (H01), from which it is lead to rectification. The pure water-free product, ethylenechlorohydrine is removed as a distillate from the head of rectifying column (C01).
申请公布号 SK41995(A3) 申请公布日期 1997.06.04
申请号 SK19950000419 申请日期 1995.03.31
申请人 NOVACKE CHEMICKE ZAVODY, A. S. 发明人 CAMAJ VLADIMIR;SPACIR JOZEF;KOLISEK MIKULAS
分类号 C07C29/64;C07C31/36 主分类号 C07C29/64
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