发明名称 Process for the preparation of 2-n-butyl-2-ethyl-1,3-propane diol
摘要 PCT No. PCT/FI94/00273 Sec. 371 Date May 4, 1995 Sec. 102(e) Date May 4, 1995 PCT Filed Jun. 20, 1994 PCT Pub. No. WO95/00464 PCT Pub. Date Jan. 5, 1995The invention relates to a novel, technically simple but efficient and high-yield process for the preparation of 2-n-butyl-2-ethyl-1,3-propane diol from 2-ethyl hexanal and formaldehyde by using a basic alkali metal hydroxide or earth alkali metal hydroxide catalyst. In the process according to the invention, cationic or neutral phase transfer catalysts are additionally used for promoting the reaction. The correct choice of the sources of the initial material components is also essential. 2-n-butyl-2-ethyl-1,3-propane diol is used, for example, in the paint industry in the preparation of pulverous paints.
申请公布号 US5618985(A) 申请公布日期 1997.04.08
申请号 US19950381919 申请日期 1995.05.01
申请人 NESTE OY 发明人 KULMALA, KARI;ANKNER, KJELL;RINTALA, LEA
分类号 B01J23/02;B01J31/02;C07C29/38;C07C31/20;(IPC1-7):C07C27/00 主分类号 B01J23/02
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