| 摘要 |
Mercury Detection Method and Apparatus utilizes cartridges including gold for adsorbing mercury as an amalgam. The adsorbed mercury is desorbed by heating and passed through a Cold Vapour Atomic Fluorescence Spectrophotometer. Each cartridge is flushed with an inert gas, so that air and contaminants are never passed directly through the detector, so only inert gas passes through it. To further prevent adsorption of contaminants, the cartridges are maintained at a minimum temperature, above ambient temperature and below 100 DEG C. To enable unattended calibration, a permeation source is provided having a permeation chamber and a valve assembly, including 3 separate valves, to ensure that in an off state mercury vapour cannot leak to the cartridges. To ensure an efficient use of the inert gas, its flow can be adjusted between 3 different levels, for flushing, desorption of mercury, and an idle state to maintain the apparatus purged air.
|
