发明名称 SAMPLE EMBEDDING BODY AND PRODUCTION THEREOF
摘要 PROBLEM TO BE SOLVED: To form an ultrathin cut piece suitable for quality inspection using a transmission microscope(TEM) efficiently while suppressing the delamination of a magnetic metal layer by adding fine particles to a resin for embedding a magnetic tape. SOLUTION: An epoxy resin is admixed with DDS and MNA at a specified ratio and stirred under normal temperature and then admixed with DMP and stirred. Subsequently, it is admixed with SiO2 powder (mean particle size; 0.01μm) by a very small quantity at a time and stirred to produce a dissolved embedding resin 4 containing fine particles. The dissolved resin 4 is poured into a molding die and the surface is flattened before being cured. A magnetic tape (sample) comprising a resin film (PET) layer 3a and a magnetic layer 3b of deposited metal is then mounted thereon with the magnetic layer 3b facing the resin 4. Finally, a resin 5 containing no fine particle of SiO2 is fed thereon and cured to form a sample embedding body. The magnetic layer 3b is not stripped off from the PET layer 3a or resin 4 at the time of dicing ultrathin cut pieces and an ultrathin cut piece (TEM sample) suitable for quality inspection can be obtained.
申请公布号 JPH0921735(A) 申请公布日期 1997.01.21
申请号 JP19950169764 申请日期 1995.07.05
申请人 KAO CORP 发明人 ISHIKAWA JUNKO;KITAORI NORIYUKI;YOSHIDA OSAMU;SASAKI KATSUMI
分类号 G01N1/36;G11B5/84;(IPC1-7):G01N1/36 主分类号 G01N1/36
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