发明名称 |
Preparation of sulfur-containing organosilicon compounds |
摘要 |
The present invention relates to a process for the production of organosilicon compounds of the formulaZ-Alk-Sn-Alk-Z(I)in which Z is selected from the group consisting of <IMAGE> where R1 is an alkyl group of 1 to 4 carbon atoms, cyclohexyl or phenyl; R2 is alkoxy of 1 to 8 carbon atoms, or cycloalkoxy of 5 to 8 carbon atoms; Alk is a divalent hydrocarbon of 1 to 18 carbon atoms and n is an integer of 2 to 8; comprising reacting (A) a compound of the formula:Z-Alk-X(II) when X is Cl or Br; with (B) an ammonium hydrosulfide or alkali metal hydrosulfide and (C) sulfur; wherein the reaction is conducted in the presence of a phase transfer catalyst and an aqueous phase.
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申请公布号 |
US5583245(A) |
申请公布日期 |
1996.12.10 |
申请号 |
US19960611866 |
申请日期 |
1996.03.06 |
申请人 |
THE GOODYEAR TIRE & RUBBER COMPANY |
发明人 |
PARKER, DANE K.;SINSKY, MARK S. |
分类号 |
B01J31/02;C07B45/06;C07B61/00;C07F7/18;(IPC1-7):C07F7/08 |
主分类号 |
B01J31/02 |
代理机构 |
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代理人 |
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主权项 |
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地址 |
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