发明名称 Magnesium doped beta -aluminum titanate thin film coating
摘要 MgxAl2-2xTi1+xO5 (x</=0.2) protective coatings have been developed for both dense and porous substrates, such as SiC and Si3N4, using a chemical solution processing method involving the hydrolysis and condensation of magnesium, aluminum and titanium precursors. The solution viscosities, pH values, H2O/alkoxide molar ratios, and dip coating withdrawal rates which are optimum for crack-free MgxAl2-2xTi1+xO5 (x</=0.2) are 1.0 to 6.2 cP, pH 1-4.5, molar ratio 1.5-10, and withdrawal rate of 2.2-8.0 cm/min, respectively. Conversion of the amorphous coating to crystalline MgxAl2-2xTi1+xO5 (x</=0.2) is achieved by a succession of calcination below 450 DEG C. and a final heat treatment above 1000 DEG C. for ten hours with controlled heating and cooling rates.
申请公布号 US5565245(A) 申请公布日期 1996.10.15
申请号 US19950396242 申请日期 1995.03.01
申请人 VIRGINIA TECH INTELLECTUAL PROPERTIES, INC. 发明人 SUN, TAWEI;BROWN, NANCY R.;BROWN, JR., JESSE J.;KANG, MIN
分类号 C01G23/00;C04B41/50;C04B41/87;C23C18/12;(IPC1-7):B05D1/18 主分类号 C01G23/00
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