发明名称 METHOD OF CONTINUAL MANUFACTURE OF 2-MERCAPTOBENZOTHIAZOLE
摘要 2-mercaptobenzothiazole prepared from aniline, carbon disulphide and sulphur in the molar ratio of from 1 : 0,9 to 1,5 : 0,85 to 1,2, with side convertibile components which accompany the synthesis with or without recycle, under pressures of from 8 to 15 MPa and at a temperature of from 130 to 200 degrees of Celsius behind a preheating zone and 130 to 300 degrees of Celsius in a reaction zone. Active components react in three to ten, advantageously in four subsequent stages, which are mutually differentiated by the temperature on the heat carrier side, whereby the temperature on the heat carrier side in the single stages has, with an increasing stage number, a decreasing tendency. The reaction is carrying out in a cascade of independently heated tubular bodies.
申请公布号 SK278229(B6) 申请公布日期 1996.05.08
申请号 SK19930000537 申请日期 1993.05.26
申请人 PODMANICKY STANISLAV;KACANI STANISLAV;KRISTOFCAK JOZEF;RISKA MILOSLAV;HANUS MILAN;VAZAN PETER;LESKA STEFAN;KRSKA STEFAN;ZELENY OTTO 发明人 PODMANICKY STANISLAV;KACANI STANISLAV;KRISTOFCAK JOZEF;RISKA MILOSLAV;HANUS MILAN;VAZAN PETER;LESKA STEFAN;KRSKA STEFAN;ZELENY OTTO
分类号 C07D277/72;(IPC1-7):C07D277/72 主分类号 C07D277/72
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