发明名称 |
METHOD FOR RECOVERING LACTIDE FROM POLYLACTIC ACID PRODUCT |
摘要 |
<p>PURPOSE:To recover a lactide useful for a monomer for polymerization raw material from a polylactic acid product in a short time, in high yield at low cost by heating and blending the polylactic acid product by a screw type extruder in the presence of water and a catalyst at a specific temperature. CONSTITUTION:(A) A polylactic acid product such as filmy sheet or hollow container obtained from a cyclic dimer such as lactic acid or a lactide as a raw material is heated and blended by a screw type extruder in the presence of (B) water and (C) a catalyst such a an alkylaluminum, zinc oxide or manganese acetate at 200-400 deg.C hydrolyzed and depolymerized to recover the objective lactide from the component A. The amounts of the components B and C used are preferably 0.1-5.0 pts.wt. of the component B and 0.1-1.0wt.% of the component C based on the amount of the component A.</p> |
申请公布号 |
JPH07309863(A) |
申请公布日期 |
1995.11.28 |
申请号 |
JP19940103091 |
申请日期 |
1994.05.17 |
申请人 |
JAPAN STEEL WORKS LTD:THE |
发明人 |
MIYOSHI RIKA;SAKAI TADAKI;HASHIMOTO NORIAKI;SUMIHIRO YUKIHIRO;YOKOTA KAYOKO |
分类号 |
C07D319/12;C08G63/06;C08G63/91;(IPC1-7):C07D319/12 |
主分类号 |
C07D319/12 |
代理机构 |
|
代理人 |
|
主权项 |
|
地址 |
|