发明名称 |
Process for reducing the free aldehyde content in N-alkylol amide monomers |
摘要 |
In a process for the preparation of N-alkylol amide monomers wherein a polymerizable amide is reacted with an aldehyde, the improvement which comprises adjusting the pH of the resulting N-alkylol amide monomer to pH 10-11 and adding thereto an alkali or alkali earth metal borohydride at a temperature of -10 DEG to 20 DEG C. so as to convert the residual free aldehyde in the equilibrium mixture to the corresponding alcohol.
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申请公布号 |
US5415926(A) |
申请公布日期 |
1995.05.16 |
申请号 |
US19930023268 |
申请日期 |
1993.02.25 |
申请人 |
NATIONAL STARCH AND CHEMICAL INVESTMENT HOLDING CORPORATION |
发明人 |
LEIGHTON, JOHN C.;CHANDRAN, RAMA S. |
分类号 |
C07B63/02;A61L15/24;C07C231/12;C07C235/28;C08F6/00;C08K5/20;D04H1/64;D06M11/80;D06M15/29;D06M15/333;D06M15/693;D21H17/36;D21H17/39;(IPC1-7):D04H1/64 |
主分类号 |
C07B63/02 |
代理机构 |
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代理人 |
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主权项 |
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地址 |
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