发明名称 THE PREPARATION OF PYRAZOLE AND ITS DERIVATIVES
摘要 A process is disclosed for preparing pyrazole and its derivatives having formula (I), in which the residues R1, R2, R3 and R4 stand for hydrogen, halogen, nitro, carboxyl, sulfonyl or C-organic residues, from alpha,beta-unsaturated carbonyl compounds having formula (II) and from hydrazine or hydrazine derivatives having formula (III). The process is characterised in that an alpha,beta-unsaturated carbonyl compound having formula (II) is at first reacted without additional diluting agents with hydrazine or a hydrazine derivative having formula (III), and the thus obtained reaction mixture is reacted in an additional reaction step with a mixture of sulphuric acid and iodine or a iodineor hydrogen iodide-relasing compound.
申请公布号 CA2169380(A1) 申请公布日期 1995.03.02
申请号 CA19942169380 申请日期 1994.08.13
申请人 发明人 MERKLE, HANS RUPERT;FRETSCHNER, ERICH
分类号 C07B35/04;C07D231/12;C07D521/00;(IPC1-7):C07D231/10 主分类号 C07B35/04
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