Method for the manufacture of dialkyl dithiophosphoric acid and dialkyl phosphorochloridothionate

摘要

A continuous process for the manufacture of dialkyl dithiophosphoric acid from phosphorus pentasulfide and a lower alkanol through the use of a settling tube and a continuous process for the manufacture of dialkyl phosphorochloridothionate by chlorinating dialkyl dithiophosphoric acid with chlorine which has been diluted with an inert gas.