发明名称 Silicon nitride composite sintered body and process for producing same
摘要 PCT No. PCT/JP92/01032 Sec. 371 Date Dec. 14, 1992 Sec. 102(e) Date Dec. 14, 1992 PCT Filed Aug. 12, 1992 PCT Pub. No. WO93/04012 PCT Pub. Date Mar. 4, 1993.A composite silicon nitride sintered body formed of silicon nitride as a matrix and silicon carbide having particle sizes of 5 to 500 nm as a phase dispersed in the sintered body, wherein the total amount of dispersed silicon carbide is 1 to 40% by volume based on the sintered body, the proportion by volume of the silicon carbide dispersed in the silicon nitride particles is 5 to 99% based on the total amount dispersed, the remainder being present only in the grain boundary of the silicon nitride, and a process for producing a silicon nitride composite sintered body which includes the steps of adding a sintering aid to amorphous composite powders as starting materials consisting of silicon, nitrogen and carbon to form a green compact; firing the green compact in a nitrogen atmosphere at 1350 DEG to 1650 DEG C. as the primary sintering; firing the same at 1600 DEG to 1900 DEG C. as the secondary sintering; and firing the same at 1800 DEG to 2200 DEG C. to transfer the silicon carbide precipitated in the particles of silicon nitride to the grain boundaries thereof.
申请公布号 US5352641(A) 申请公布日期 1994.10.04
申请号 US19920956887 申请日期 1992.12.14
申请人 SUMITOMO ELECTRIC INDUSTRIES, LTD. 发明人 MATSUI, JIN-JOO;YAMAKAWA, AKIRA
分类号 C04B35/584;(IPC1-7):C04B35/58 主分类号 C04B35/584
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