发明名称 METHOD FOR MANUFACTURING NEW-2-AMINE-4,6-DICHLOR-5-METHYL PHENOL
摘要 Method of producing new derivatives of 2-amino-4,6-dichloro-5-methylphenol with general formula 1, where R1 and R2 are hydrocarbon chains with 1-2 carbon atoms in the case of R1 and 5-10 carbon atoms in the case of R2, characterized in that 4-alkylphenoxycarboxylic acid with general formula 2, where R1 and R2 have the meanings given above, is converted using thionyl chloride to its chloride, which is then subjected to a condensation reaction with 2-amino-4,6-dichloro-5-methylphenol, where the condensation reaction takes place in a water-solvent medium, the solvents being hydrophobic aromatic hydrocarbons and/or halogenous derivatives, and after completion of condensation an organic layer is separated, from which, after the oleaginous solvents have been distilled off, the remainder is recrystallized from n-hexane or petrol with a boiling point of 60-100 degrees C.<IMAGE>
申请公布号 PL162038(B2) 申请公布日期 1993.08.31
申请号 PL19900287361 申请日期 1990.10.17
申请人 INSTYTUT BARWNIKOW I PRODUKTOW ORGANICZNYCH 发明人 WYREBSKA LUCJA;KACZMAREK WITOLD;ZIMNICKI JAN;STAWSKA HALINA;STASIAK JAN;CISLO ROMAN
分类号 C07C215/74;C07C235/24;C07C235/42;(IPC1-7):C07C235/24 主分类号 C07C215/74
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