发明名称 Method of manufacturing vitamin D2, Vitamin D3, activated type vitamin D2, activated type vitamin D3, and their derivatives
摘要 There is provided a method with which vitamin D2, vitamin D3, activated type vitamin D2, activated type vitamin D3 and their derivatives are prepared from 7,8 -dihyroxy vitamin D2, D3 or any of their derivatives by means of a reducing elimination technique involving as cyclic orthoester of a 7,8-dihydroxy compound or a thiocarbonate compound as an intermediate compound or an elimination technique utilizing a reducing metal such as titanium. The method according to the invention ensures a practical and simple synthetic process and a high yeild as compared with any existing methods for manufacturing these chemicals.
申请公布号 US5225579(A) 申请公布日期 1993.07.06
申请号 US19920873887 申请日期 1992.04.24
申请人 HOXAN CORPORATION 发明人 TAHARA, YUJI
分类号 C07C401/00 主分类号 C07C401/00
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