发明名称 FOERFARANDE FOER FRAMSTAELLNING AV AMYL-2-ANTRAKINON FRAON AMYLBENSEN OCH FTALSYRAANHYDRID
摘要 1. Process for manufacturing 2-amylanthraquinone having a high content of the tert-isomer, by reaction of phthalic anhydride with tert-amylbenzene in the presence of a catalyst consisting of a mixture of hydrofluoric acid and boron trifluoride, followed by conversion of the amyl-orthobenzoylbenzoic acid obtained to 2-amylanthraquinone according to processes which are known per se, characterized in that the reaction of phthalic anhydride with tert-amylbenzene is performed at a temperature of between -60 C and -20 C in a two-phase liquid reaction medium formed as a result of the presence of a solvent for tert.amylbenzene which is inert and immiscible with the mixture of hydrofluoric acid and boron trifluoride under the conditions of the reaction.
申请公布号 FI87189(C) 申请公布日期 1992.12.10
申请号 FI19850004220 申请日期 1985.10.28
申请人 ATOCHEM, 发明人 DEVIC,MICHEL
分类号 C07C50/16;B01J27/12;C07C45/00;C07C46/00;C07C50/18;C07C67/00 主分类号 C07C50/16
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