发明名称 NMR-SPECTROMETER WITH SAMPLE EXCHANGER
摘要 PCT No. PCT/DE89/00324 Sec. 371 Date Nov. 21, 1990 Sec. 102(e) Date Nov. 21, 1990 PCT Filed May 20, 1989 PCT Pub. No. WO89/11646 PCT Pub. Date Nov. 30, 1989.In order to take NMR-spectrograms, it is necessary that the spins of the sample be arranged in a homogeneous magnetic field. For that purpose, NMR-spectrometers have a magnet arrangement (2) in the magnetic field of which is arranged a sampling head (5). When the spin-lattice-relaxation time T1 of substances to be examined lies in the range of hours, the spectrometer is unusable for hours due to the necessary prepolarization of the sample. The invention is aimed at solving this problem. A sample magazine (11) is arranged in the magnetic field generated by the magnet arrangement (2). It offers the possibility of exposing a larger number of samples to the magnetic field of the magnet (2) while simultaneously carrying out measurements. Since measurements of samples having long spin-lattice-relaxation times T1 require a considerable time, the capacity of a magazine arranged in the magnetic field is sufficient to ensure a practically continuous operation of the spectrometer, even when samples with long T1 are analysed. The design of the sample magazine (11) as a rotatable drum (21) arranged in the bore ( 1) of a cryomagnet is particularly appropriate for cryomagnets.
申请公布号 US5150054(A) 申请公布日期 1992.09.22
申请号 US19900602314 申请日期 1990.11.21
申请人 BRUKER ANALYTISCHE MESSTECHNIK GMBH 发明人 DUPREE, RAYMOND
分类号 G01R33/30 主分类号 G01R33/30
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