发明名称 Preparation of halohydroxypropyl-trialkylammonium halides
摘要 The present invention is a process for producing halohydroxypropyltrialkylammonium halides by reacting a trialkylamine salt with an epihalohydrin, the improvement comprising using 1,3-dihalo-2-propanol as a cosolvent. Using that cosolvent reduces the amount of diquaternary, dichloropropanol, and epoxy by-products formed. The cosolvent is preferably separated from the reaction mixture and recycled for use with additional trialkylamine salt and epihalohydrin. The process is particularly useful in preparing chlorohydroxypropyltrimethylammonium chloride.
申请公布号 US5077435(A) 申请公布日期 1991.12.31
申请号 US19900580988 申请日期 1990.09.12
申请人 THE DOW CHEMICAL COMPANY 发明人 KIMBRELL, RUSSELL B.;KNEUPPER, CHRISTIAN D.;KRAUSE, RUBEN L.
分类号 C07C215/90 主分类号 C07C215/90
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