摘要 |
PURPOSE:To prevent the generation of a crack from a pin hole and the redidue of deflection and wripple, by joining a precious metal to be made for foil with its hot compression with its superposition with copper or silver after executing a hot treatment in advance thereon and making a precious metal foil with an acid treatment thereafter. CONSTITUTION:A prepressurization is performed by superposing with a material Cu after performing a heat treatment in the atmosphere on a material Pt, a heat treatment is performed under the atmosphere of nitrogen and hydrogen thereafter, the compression joining is executed by performing a normal pressurization after taking it out of a furnace and rolling is executed in the front and back, right and left and diagonal directions with a roll rolling mill thereafter. A heat treatment is then performed in a conveyor furnace under nitrogen and hydrogen, rolling is executed further and thereafter cupper is removed with a nitric acid solution and a Pt foil is obtd. |