发明名称 PROCESS TO SYNTHESIZE AB-PBO MONOMER AND PHOSPHATE SALTS THEREOF
摘要 AB-polybenzoxazole monomer, such as 3-amino-4-hydroxybenzoic acid, can be synthesized in high yields from a hydroxy-benzoic acid or related compound in a three-step process of (1) nitration, (2) hydrolysis of the ester, and (3) reduction of the nitro moiety. The monomer is conveniently recovered as a phosphate salt in high purity by precipitating and recrystallizing from a phosphoric acid solution.
申请公布号 AU5956990(A) 申请公布日期 1991.02.22
申请号 AU19900059569 申请日期 1990.07.03
申请人 THE DOW CHEMICAL COMPANY 发明人 WILLIAM J. HARRIS;CARL W. HURTING;ZENON LYSENKO
分类号 C07C227/04;C07C227/06;C08G73/22 主分类号 C07C227/04
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