发明名称 PROCESS FOR THE PREPARATION OF MESOPHASE PITCHES
摘要 <p>. of the Disclosure A process for the preparation of an excellent mesophase pitch suitable for use as a spinning pitch for the production of high performance carbon fibers is disclosed. The mesophase pitch can satisfy the four remarkable characteristics at the same time, i.e., a softening point of below 320.degree.C as determined by Mettler method, a mesophase content of above 90% as examined on a polarized microscope, a quinoline insoluble content of less than 20%, and a xylene soluble content of less than 20%. The mesophase pitch is particularly homogeneous and is easily spinnable. The process can be characterized by a preliminary extraction step, a continuous heat treatment step, and an extraction step. In some cases, the preliminary extraction step can be omitted. Graphite fibers having a tensile strength of about 400 Kg/mm2 and a modulus of elasticity of above 60 ton/mm2 can be obtained from the mesophase pitch. Further, even carbon fibers prepared at a carbonization temperature of 1000.degree.C have a tensile strength of about 300 Kg/mm2.</p>
申请公布号 CA1264692(A) 申请公布日期 1990.01.23
申请号 CA19870536809 申请日期 1987.05.11
申请人 IIZUKA KOZO;MARUZEN PETROCHEM CO LTD;AGENCY IND SCIENCE TECHN 发明人 TSUCHITANI, MASATOSHI;NAITO, SAKAE;NAKAJIMA, RYOICHI
分类号 C10C3/02;C10C1/16;C10C1/18;C10C1/19;C10C3/00;C10C3/04;C10C3/08;C10C3/10;D01F9/145;D01F9/15;D01F9/155;(IPC1-7):C10C3/00 主分类号 C10C3/02
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