发明名称 Process for the preparation of hydroxybenzaldoxime O-ethers
摘要 A process for the preparation of a hydroxybenzaldoxime O-ether of the formula <IMAGE> (I) in which R1 represents alkyl, comprising (a) in a first step, hydrogenating a nitro-benzaldoxime O-ether of the formula <IMAGE> (II) using the calculated amount of hydrogen in the presence of a catalyst and in the presence of a diluent, and (b) in a second step, reacting the amino-benzaldoxime O-ether of the formula <IMAGE> (III) thus obtained with a diazotizing agent in acidic, aqueous solution, and, without isolation, thermally hydrolyzing the resultant diazonium salt of the formula <IMAGE> (IV) in which X(-) represents an equivalent of an inorganic anion, in acidic, aqueous solution.
申请公布号 US4845288(A) 申请公布日期 1989.07.04
申请号 US19880147417 申请日期 1988.01.25
申请人 BAYER AKTIENGESELLSCHAFT 发明人 LANTZSCH, REINHARD;ZIEMANN, HEINZ;ELBE, HANS-LUDWIG
分类号 C07C251/48;A01N43/653;A61K31/41;C07B61/00;C07C67/00;C07C239/00;C07C249/12;C07C251/32;C07D249/08 主分类号 C07C251/48
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