发明名称 METHOD OF SYNTHESIS OF PHTHALIMIDE
摘要 organic chemistry, chemical technology. SUBSTANCE: invention relates to technology of synthesis of phthalimide used as a parent raw in production of N-(cyclohexylthio)phthalimide, anthranilic acid, different products if fine organic synthesis and a special addition in nickel plating. New aspect of the proposed method involves interaction at 114-119.5 C under excessive pressure from 0.05 to 0.7 ati and in the mole ratio phthalic anhydride : urea in the range = 1.0 : (0.67-0.95) in an organic solvent medium, among them, taken from the group: coal xylene, petroleum xylene, ortho-xylene, meta-xylene, para-xylene, ethylbenzene taken in the amount 230-300% of the parent phthalic anhydride used. EFFECT: improved method of synthesis. 3 cl, 1 tbl
申请公布号 RU2185376(C1) 申请公布日期 2002.07.20
申请号 RU20010100145 申请日期 2001.01.03
申请人 VOLGOGRADSKOE OTKRYTOE AKTSIONERNOE OBSHCHESTVO "K;VOLG AOOT K 发明人 PODDUBNYJ I.S.;KUZNETSOV A.A.;GURA L.N.;SERGEEV S.A.;KOSOV I.JU.
分类号 C07D209/48;(IPC1-7):C07D209/48 主分类号 C07D209/48
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