发明名称 GLOW DISCHARGE EMISSION SPECTRAL ANALYZER
摘要 PURPOSE:To stabilize an analysis by providing a feedback system which detects the internal resistance of a glow discharge tube using a sample as a cathode and maintains the internal resistance of the glow discharge tube at approximately a constant level and maintaining a sputtering rate automatically at a constant value. CONSTITUTION:Gaseous argon is admitted through an inflow port 5 into the glow discharge tube G and is discharged from outflow ports 6 and 7. A flow rate control valve V is otherwise inserted into, for example, a gaseous argon supply pipe and the voltage drop generated across a resistor (r) connected in series to the discharge tube G is detected by a current detector D to control a valve driving device P via a comparator C, thereby opening and closing the valve V. The internal resistance of the discharge tube G increases and the tube current increases when the sputtering rate of the sample is low. The valve V is then opened to increase the gaseous argon pressure, by which the internal resistance is decreased and the sputtering rate is maintained constant. The stable analysis is thereby executed.
申请公布号 JPS63210751(A) 申请公布日期 1988.09.01
申请号 JP19870044185 申请日期 1987.02.27
申请人 SHIMADZU CORP 发明人 FUKUI ISAO;MIYAMA TAKAO
分类号 G01N21/67 主分类号 G01N21/67
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