发明名称 |
METHOD FOR PRODUCING AMMONIUM PARATUNGSTATE |
摘要 |
<p>A method is disclosed for producing relatively pure ammonium paratungstate from an impure tungsten solution. The method involves first adding hexamethylenetetramine to the tungsten solution and adjusting the pH to from about 1.0 to about 2.0 with a mineral acid to form a first precipitate of a tungsten hexamethylenetetramine product, which is then separated from its mother liquor. The precipitate is then slurried in water and the pH adjusted to from about 7.0 to about 8.5 with ammonia to dissolve the precipitate. The resulting solution is then adjusted to from about 1.0 to about 2.0 with a mineral acid to form a second precipitate of the tungsten hexamethylenetetramine product which is then separated from its mother liquor. The second precipitate is then slurried in a solution of water and sufficient ammonia to form ammonium paratungstate which crystallizes out on evaporation of the slurry. The ammonium paratungstate is then separated from its mother liquor.</p> |
申请公布号 |
GB2172588(B) |
申请公布日期 |
1988.05.05 |
申请号 |
GB19860006934 |
申请日期 |
1986.03.20 |
申请人 |
* GTE PRODUCTS CORPORATION |
发明人 |
RICHARD A * SCHEITHAUER;CLARENCE D * VANDERPOOL;MICHAEL J * MILLER |
分类号 |
C01G41/00;C22B3/28;(IPC1-7):C01G41/00;C01C1/28 |
主分类号 |
C01G41/00 |
代理机构 |
|
代理人 |
|
主权项 |
|
地址 |
|