发明名称 |
PRODUCTION OF AQUEOUS SOLUTION OF CATIONIC THERMOSETTING RESIN |
摘要 |
PURPOSE:To obtain the titled aqueous solution having high solid concentration and excellent effect to improve paper strength in wet state, by reacting a polyalkylenepolyamine with an aliphatic dicarboxylic acid at a specific ratio and reacting the resultant polyamide polyamine with a specific amount of epichlorohydrin. CONSTITUTION:A polyalkylenepolyamine (e.g. diethylenetriamine) is mixed with an aliphatic dicarboxylic acid (e.g. oxalic acid) at a molar ratio of 1.0:(0.9-1.1) and subjected to dehydrative condensation by heating at 135-150 deg.C to obtain a polyamide polyamine having a viscosity of 300-600cps measured by Brookfield viscometer as 50% aqueous solution. An aqueous solution of the polyamide polyamine having a concentration of 20-50% is mixed with 1.2-2.0 equivalent of epichlorohydrin based on the amino group of the polyamide polyamine and the components are made to react with each other until the viscosity of 20% aqueous solution of the product reaches 30-200cps (measured under the above condition) to obtain the objective aqueous solution. The solution is useful as a fixing resin for wet paper strengthening agent, sizing agent and filler. |
申请公布号 |
JPS6369826(A) |
申请公布日期 |
1988.03.29 |
申请号 |
JP19860213781 |
申请日期 |
1986.09.12 |
申请人 |
DICK HERCULES KK |
发明人 |
KONDO KAORU;KOSUGE MASANORI;OKAMOTO JUNKO |
分类号 |
C08G69/48;D21H17/55;D21H17/56 |
主分类号 |
C08G69/48 |
代理机构 |
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代理人 |
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主权项 |
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地址 |
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