发明名称 |
Process for producing 1,2-substituted imidazoline compounds |
摘要 |
A 1,2-substituted imidazoline compound having the formula (I): <IMAGE> (I) in which R2 is an alkyl or alkenyl group having 8 to 22 carbon atoms and n is 2 or 3, is produced by (1) feeding in a reactor a dialkylenetriamine (II) with a higher fatty acid of R2COOH or an ester thereof (III) at a molar ratio of the compound (III) to the compound (II) in the range of 1.5:1 to 1.8:1, (2) effecting the reaction at an internal temperature of 100 DEG to 250 DEG C. at a reduced pressure, (3) adding to the reaction mixture so that the above defined molar ratio in total may reach at least 2.0:1 and (4) continuing the reaction at an internal temperature of 100 DEG to 250 DEG C. at a reduced pressure. The reaction proceeds with a high yield of the product (I), without by-production to primary and second amines.
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申请公布号 |
US4709045(A) |
申请公布日期 |
1987.11.24 |
申请号 |
US19860871651 |
申请日期 |
1986.06.06 |
申请人 |
KAO CORPORATION |
发明人 |
KUBO, MAKOTO;SOTOYA, KOSHIRO;OKABE, KAZUHIKO |
分类号 |
C07D233/16;C07D233/06;(IPC1-7):C07D233/04 |
主分类号 |
C07D233/16 |
代理机构 |
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代理人 |
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主权项 |
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地址 |
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