发明名称 Preparation of cafestol.
摘要 A process for the preparation of cafestol from kahweol wherein the kahweol is hydrogenated in the presence of a partially deactivated palladium catalyst on a calcium carbonate or active carbon support conditioned by lead as well as a process for preparing a mixture of cafestol and kahweol wherein coffee oil is treated with anhydrous methanol in the presence of a basic catalyst, the reaction medium is diluted with a substantially water-insoluble solvent which dissolves the formed methyl esters and then extracted with aqueous methanol, the aqueous methanol phase then being separated and then further extracted with a low-boiling chlorinated hydrocarbon which is then separated from the aqueous methanol phase and evaporated to give the mixture of cafestol and kahweol.
申请公布号 EP0239730(A1) 申请公布日期 1987.10.07
申请号 EP19870100868 申请日期 1987.01.22
申请人 SOCIETE DES PRODUITS NESTLE S.A. 发明人 BERTHOLET, RAYMOND
分类号 C07B61/00;B01J23/04;B01J27/00;B01J27/232;C07D307/77;C07D307/93;(IPC1-7):C07D307/93;A23F5/48 主分类号 C07B61/00
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