发明名称 |
Process for the preparation of methyl carbamates and thioimidates |
摘要 |
A continuous, close-coupled method for making N-methyl carbamate pesticides which comprises contacting the methyl isocyanate in a vapor phase mixture containing methyl isocyanate and water with a selected oxime or phenol, said mixture being the reaction product formed by oxidizing monomethylformamide. An optional intermediate step for preparing the methyl isocyanate/water vapor phase reaction mixture for contact with the oxime or phenol is to remove therefrom a portion of the water without liquefying the methyl isocyanate by cooling the mixture to a temperature below the dew point of water but above the dew point of the methyl isocyanate.
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申请公布号 |
US4698438(A) |
申请公布日期 |
1987.10.06 |
申请号 |
US19860827517 |
申请日期 |
1986.02.11 |
申请人 |
E. I. DU PONT DE NEMOURS AND COMPANY |
发明人 |
BLAISDELL, CHARLES T.;CORDES, WALTER J.;HEINSOHN, GEORGE E.;KOOK, JOHN F.;KOSAK, JOHN R. |
分类号 |
A01N47/10;A01N47/22;A01N47/24;C07C;C07C263/12;C07C269/02;C07C271/06;C07C271/12;C07D307/78;C07D307/84;C07D307/86;C07D317/18;C07D317/20;C07D317/24;C07D317/46;C07D317/64;(IPC1-7):C07C119/18;C07C131/00;C07C125/04 |
主分类号 |
A01N47/10 |
代理机构 |
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代理人 |
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主权项 |
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地址 |
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