发明名称 High strength, melt spun carbon fibers and method for producing same.
摘要 <p>Hollow carbon fibers and carbon fibers having a generally C-shaped transverse cross-sectional area (see Fig. 7) are produced by extruding a carbon­aceous anisotropic liquid precursor through a spinneret (14) having a capillary with a generally C-shaped cross-sectional area, into a fiber filament, controlling the viscosity of the molten precursor, the pressure of the molten precursor and the linear take-up speed of the filament to yield a fiber filament having a cross-sectional area shaped substantially like the shape of the cross-sectional area of the capillary and further having a line-origin microstructure, rendering the filament infusible, heating the filament in an inert pre-carbonizing environment at a temperature in the range of 600°C to 1000°C for 1 to 5 minutes, and heating the filament in an inert carbonizing environment at a temperature in the range of 1550°C to 1600°C for 5 to 10 minutes, to substantially increase the tensile strength of the filament. The carbon fiber filament so produced has a line-origin microstructure in which the origin line is located and shaped substantially as a line which constitutes the line formed by uniformly collapsing the perimeter of the transverse cross-sectional area of the fiber filament upon itself. The carbon fiber filament has a tensile strength greater than 200 ksi and as high as the 700 to 800 ksi range, yet a modulus of elasticity on the order of 25-35 msi. The top to bottom outside diameter of the fiber's transverse cross-sectional area is on the order of 30 to 50 microns, and the wall thicknesses are on the order of 8 to 15 microns. </p>
申请公布号 EP0232051(A2) 申请公布日期 1987.08.12
申请号 EP19870300460 申请日期 1987.01.20
申请人 CLEMSON UNIVERSITY 发明人 FAIN, CHARLES C.;EDIE, DANNY DALE
分类号 D01D5/253;D01F9/14;D01F9/145;D01F9/155;D01F9/22;D01F9/32;(IPC1-7):D01F9/22 主分类号 D01D5/253
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