发明名称 |
Process for the preparation of diazocyano acids by reacting keto-acids with cyanogen compounds |
摘要 |
A process for the preparation of a diazocyano acid, which comprises reacting a keto-acid or its sodium salt with a cyanogen compound such as sodium cyanide or hydrogen cyanide and a hydrazine in water to form a concentrated aqueous solution of a hydrazo compound, adding acetone and/water to the concentrated aqueous solution to form a solution of the hydrazo compounds, adding chlorine gas to the solution to oxidize the hydrazo compound and form a diazocyano acid, adding acetone to the obtained reaction mixture during or after the oxidation if necessary, and separating and recovering the supernatant layer of the acetone-water solution containing the diazocyano acid from the mixture.
|
申请公布号 |
US4684718(A) |
申请公布日期 |
1987.08.04 |
申请号 |
US19840676265 |
申请日期 |
1984.11.29 |
申请人 |
UBE INDUSTRIES, LTD. |
发明人 |
ASHITAKA, HIDETOMO;JINDA, KAZUYA;MIWA, YOSHIYUKI |
分类号 |
C07C255/65;C08F4/04;(IPC1-7):C07C101/26;C07C107/02;C08G63/68 |
主分类号 |
C07C255/65 |
代理机构 |
|
代理人 |
|
主权项 |
|
地址 |
|