| 摘要 |
1,3-Bis(3-aminophenoxy)-5-halogenobenzene (I)[X=chloride, bromine! is prepd. for use as insecticide or solvent. 1,3, 5- Trihalogenobenzene is reacted with 3-aminophenol to give the compd. (I). The reaction solvent is aprotic polar solvent, such as N-methyl formamide, dimethylsulfoxide, hexamethylphosphoric triamide. The reaction medium contains dehalogenating agent, such as hydride, corbonate salt, alkalimetal alkoxide. This reaction is performed at 120-240≰C.
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