发明名称 Process for the preparation of 1,4-diamino-2,3-dicyanoanthraquinone
摘要 The invention relates to a process for the preparation of 1,4-diamino-2,3-dicyanoanthraquinone, starting from 1,4-diaminoanthraquinones, or salts thereof, of the formula <IMAGE> wherein n is 0, 1 or 2. To introduce the two cyanide radicals, the starting material is treated, in the presence of an oxidizing agent, with a compound which donates cyanide ions. The process comprises using as solvent a mixture of a carboxamide, an N-alkylated carboxamide or a lactam and water, which mixture contains more than 10% by weight of water. 1,4-Diamino-2,3-dicyanoanthraquinone is an important intermediate for the synthesis of textile dyes.
申请公布号 US4661292(A) 申请公布日期 1987.04.28
申请号 US19850784434 申请日期 1985.10.03
申请人 CIBA-GEIGY CORPORATION 发明人 SCHAULIN, RUDOLF;GRELAT, MAURICE
分类号 C07C309/53;C07C67/00;C07C255/58;C07C301/00;C07C303/22;(IPC1-7):C07C143/665;C07C97/24 主分类号 C07C309/53
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