发明名称 Process for preparing spherulitic crystals of high bulk density and packing density, in particular of spherically crystalline nitroguanidine
摘要 Spherulitic crystals, such as spherical nitroguanidine, are prepared by super cooling and stirring a hot saturated solution in dipolar aprotic solvents at a specific stirring rate epsilon </= 0.1 W/kg, adding seeding grains of the same substance of at most 50 mu m, the addition of seeding grains being carried out prior to the temperature being reached at which self-nucleation begins. Instead of the addition of seeding grains, spherulitic crystals can also be obtained at the same stirring rate by addition of polar ionically active substances or by addition of organic acids.
申请公布号 DE3527200(A1) 申请公布日期 1987.03.19
申请号 DE19853527200 申请日期 1985.07.30
申请人 HOMMEL,HORST,DIPL.-ING. 发明人 HOMMEL,HORST,DIPL.-ING.
分类号 B01D9/02;C06B21/00;C06B25/34;(IPC1-7):B01D9/02;C07C129/10 主分类号 B01D9/02
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