发明名称 PROCESS FOR THE PREPARATION OF CRYSTALLINE SODIUM PHENYLPYRUVATE MONOHYDRATE
摘要 The invention concerns a process for preparation of crystallized monohydrated sodium phenylpyruvate comprising: hot reacting benzaldehyde in an aqueous medium in the presence of a catalytic quantity of ethanolamine with the stoichiometric quantity of hydantoin, then treating the reactional medium hot at pH=14 through an excess of sodium hydroxide, acidifying to pH=9 with concentrated hydrochloric acid the so obtained solution and separating the formed precipitate.
申请公布号 DE3461029(D1) 申请公布日期 1986.11.27
申请号 DE19843461029 申请日期 1984.07.12
申请人 SOCIETE FRANCAISE HOECHST SOCIETE ANONYME DITE: 发明人 SCHOUTEETEN, ALAIN;CHRISTIDIS, YANI
分类号 C07C59/84;B01J31/00;B01J31/02;C07B61/00;C07C51/00;C07C51/41;C07C67/00;(IPC1-7):C07C59/84 主分类号 C07C59/84
代理机构 代理人
主权项
地址