发明名称 |
Method for the fractionation of reactive terminated polymerizable oligomers |
摘要 |
Acetylene or vinyl-terminated polymerizable oligomers of polyamic acid are fractionated to obtain an oligomer product having a molecular weight in the range of 2,000 to 4,000 which exhibits improved wetting and film forming properties. Fractionization is accomplished by dissolving the unfractionated polymerizable oligomer in a solvent in which the desired molecular weight fraction is soluble. The oligomer solution is passed through a filter which removes undissolved material having a molecular weight in excess of the desired molecular weight range. The filtrate is admixed with a hydrocarbon to precipitate the desired molecular weight fraction. Thereafter the collected solids can be redissolved in a ketonic solvent and the fractionation procedure repeated to further improve the molecular weight content of the fractionated oligomer.
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申请公布号 |
US4622383(A) |
申请公布日期 |
1986.11.11 |
申请号 |
US19850759630 |
申请日期 |
1985.07.26 |
申请人 |
INTERNATIONAL BUSINESS MACHINES CORPORATION |
发明人 |
ARAPS, CONSTANCE J.;KANDETZKE, STEVEN M.;TAKACS, MARK A. |
分类号 |
H01L21/312;H01L21/762;H01L23/532;H05K1/00;H05K1/03;H05K3/46;(IPC1-7):C08G69/26;C08G69/34 |
主分类号 |
H01L21/312 |
代理机构 |
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代理人 |
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主权项 |
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地址 |
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