发明名称 CONTINUOUS WET SPINNING METHOD OF PRODUCING USEFUL FILAMENTARY MATERIALS OF AN ACRYLONITRILE COPOLYMER
摘要 A continuous wet-spinning method for producing a useful filamentary material, such as multi-filaments or a tow, from a spinning solution of an acrylonitrile copolymer in an aqueous saline solvent consisting essentially of zinc chloride. In this method, an aquagel filamentary material obtained by spinning the spinning solution is taken up from an aqueous coagulating bath, continuously stretched in water and continuously dried so as to form a dried filamentary material having a moisture content of less than 5 weight percent and a transparency of at least 70 percent, measured under specific conditions. Subsequently, the dried filamentary material is continuously relaxed under a tension of at least 2 mg. per denier in substantially saturated steam at a temperature, X( DEG C), such that the following expression is satisfied: 55 log Y + 5M - 417 </= X </= 100 log Y + 5M - 434 wherein 160 DEG C </= x </= 100 DEG C, 45 percent </= Y </= 15 percent and Y is the percent of shrinkage.
申请公布号 US3689621(A) 申请公布日期 1972.09.05
申请号 USD3689621 申请日期 1970.03.02
申请人 TOHO BESLON CO. LTD. 发明人 SABURO FUJII;YASUO SAJI;KOZO YAMADA;ZENJI MAKITA;SHIGERU IKEGAMI
分类号 D01F6/18;(IPC1-7):D01F3/28 主分类号 D01F6/18
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