发明名称 MANUFACTURE OF ULTRA-FINE CARBON FIBER BY VAPOR-PHASE PROCESS
摘要 PURPOSE:To manufacture ultra-fine carbon fiber having excellent crystal orientation, in high yield and productivity, by the high-temperature reaction of a mixed gas consisting of an organic metallic compound vapor and a carrier gas. CONSTITUTION:A carrier gas is introduced through the inlet 40 to the vapor of an organic metallic compound (preferably the compound of iron, cobalt or nickel) in the evaporator 42 to obtain a mixed gas. The mixed gas is introduced through the feeding line 48 and the gas-inlet line 49 into the reaction tube 50 heated with the heater 52, and subjected to the high-temperature reaction to obtain the objective carbon fiber. The organic metallic compound is preferably the one composed solely of carbon, hydrogen and iron. The carrier gas is preferably composed of >=60% H2 gas, 3-20% gases such as He, Ar, Kr, Ne, N2, CO2, etc., and 1-6% H2S.
申请公布号 JPS6134221(A) 申请公布日期 1986.02.18
申请号 JP19840155154 申请日期 1984.07.27
申请人 NIKKISO CO LTD 发明人 ARAKAWA KOHEI
分类号 D01F9/12;D01F9/127;D01F9/133 主分类号 D01F9/12
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