发明名称 METHOD AND APPARATUS FOR FILLING OF COLUMN IN LIQUID CHROMATOGRAPH
摘要 PURPOSE:To improve separation efficiency of a subjected material, by fitting under pressure a movable plug mounted on a column inside the column with a mechanical transmission mechanism and charging the column with a filling material under pressure. CONSTITUTION:After pouring concentration adjusted slurry filling material into a column 1 fixed from above onto a supporting bench 6, a movable plug 2 is fit and further, an electric motor 5 is driven to a constant speed by setting a travelling speed of the movable plug, allowing the plug 2 to drop through reduction gear 7, rotating shafts 4A, 4B. Thus, the poured slurry of the filling material is filled under a constant load and when the set load is found in excess of the set value in the neighborhood of the completed state of filling, the motor 5 is brought to a stand still to finish up the filling operation. As a reduction ratio of the reduction gear 7 is set in a wide range for the movable plug 2 of the column, the plug 2 is not subjected to any movement by fluid pressure at the time of analysis or blelding, etc., and consequently, the column can be used as a backed column even if the pressure is approximately 200kg/cm<2>G.
申请公布号 JPS617466(A) 申请公布日期 1986.01.14
申请号 JP19840126361 申请日期 1984.06.21
申请人 SHOWA DENKO KK 发明人 KUROIWA SADAO;SAITOU ISAO;ISHIDA NORIO;YAMADA TSUYOSHI
分类号 B01D15/08;G01N30/52;G01N30/56 主分类号 B01D15/08
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