摘要 |
NEW MATERIAL:The compound of formula I (R<1>-R<3> are halogen, lower alkyl or lower alkoxy; R<1>-R<3> are not lower alkyl at the same time). EXAMPLE:2-[Trimethoxy]silyl-1,3-butadiene. USE:A silane coupling agent. PREPARATION:The 2-substituted-1,4-dihalogeno-2-butene of formula II {e.g. 1,4- dichloro-2-[trimethoxy]silyl-2-butene} is dehalogenated preferably with zinc powder in the presence of a non-alcoholic solvent such as THF.
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