发明名称 Verfahren zur Herstellung von als optische Aufheller verwendbaren Azolverbindungen
摘要 The invention comprises compounds of the formula <FORM:1072919/C2/1> and the production of compounds of the formula <FORM:1072919/C2/2> where R is a 4,41-stilbene radical, A is an o-phenylene radical and X is 0 or 5, by heating HOOC-R-COOH with HX-A-NH2.(HCl)m (where m is 0 or 1) and a halogenating agent capable of converting COOH to acid halide, e.g. POCl3, to form an intermediate condensation product, and then refluxing to form the product. A solvent may be used, e.g. 1,2,4-trichlorobenzene. Both R and/or A may be substituted; many possible substituents are given. In examples, X is 0 or S and R and A are unsubstituted; and X is 0, R is unsubstituted, and A is phenyl-substituted. The products may be mixed with soaps or detergents for increasing fabric brightness or whiteness.
申请公布号 DE1445699(A1) 申请公布日期 1968.12.05
申请号 DE19641445699 申请日期 1964.05.15
申请人 EASTMAN KODAK COMPANY 发明人 SIGMUND BLOOM,MELVIN
分类号 C07D235/20;C07D263/62;C07D277/64;D06L3/12 主分类号 C07D235/20
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