发明名称 3-CHLORO-4-FLUOROPHENYL ESTER
摘要 NEW MATERIAL:The compound of formula I [Z is group of formula II, formula III(R is 3-8C straight-chain alkyl or alkoxy), formula IV or formula V (R is 3-8C straight-chain alkyl)]. EXAMPLE:4-n-Butylbenzoic acid 3'-chloro-4'-fluorophenyl ester. USE:A liquid crystal composition having high positive dielectric anisotropy, lowered driving voltage and improved response characteristics. PREPARATION:The compound of formula I can be prepared by (1) reacting the carboxylic acid of formula VI with a halogenation agent (e.g. thionyl chloride), and (2) reacting the resultant carboxylic acid halide of formula VII (X is halogen) with 3-chloro-4-fluorophenol of formula VIII in an inert solvent (e.g. diethyl ether). Preferably, a basic substance (e.g. pyridine) is added to the inert solvent to remove the isolated hydrogen halide from the reaction system.
申请公布号 JPS59210048(A) 申请公布日期 1984.11.28
申请号 JP19830082488 申请日期 1983.05.13
申请人 SEIMI KAGAKU KK 发明人 KUMAI YUTAKA;TAKEDA KATSUHIKO;MACHIDA KATSUTOSHI
分类号 C07C67/14;C07C69/753;C07C69/773;C07C69/92;C07C69/94 主分类号 C07C67/14
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