发明名称 |
Process for the preparation of 4-chloro-2-nitrobenzonitrile. |
摘要 |
<p>4-chloro-2-nitrobenzonitrile is prepared by reacting 1 mol of 2,5-dichloronitrobenzene with 1.0 to 1.5 mols of cupper (I) cyanide, preferably in an inert solvent, for 2 to 6 hours at 140 to 170 DEG C.
<??>An inorganic cyanide may also be present.
<??>Yields of 43 to 73% are demonstrated. </p> |
申请公布号 |
EP0110559(A1) |
申请公布日期 |
1984.06.13 |
申请号 |
EP19830306539 |
申请日期 |
1983.10.27 |
申请人 |
SANWA KAGAKU KENKYUSHO CO., LTD. |
发明人 |
KURONO, MASAYASU;YAMAGUCHI, TAKUJI;USUI, TOSHINAO |
分类号 |
C07B61/00;B01J27/00;B01J27/26;C07C67/00;C07C253/00;C07C253/14;C07C255/49;C07C255/50;(IPC1-7):07C121/52;07C120/04 |
主分类号 |
C07B61/00 |
代理机构 |
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代理人 |
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主权项 |
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地址 |
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