发明名称 Process for the synthesis of an N,N-disubstituted hydrazone
摘要 In the process, a nitrosation is carried out by adding an aqueous solution of sodium nitrite to a solution which contains 1 part by weight of an N,N-disubstituted amine which is dissolved in 3 to 30 parts by weight of an organic acid, the nitrosated product is then reduced to an N,N-disubstituted hydrazine by addition of a reducing agent to the mixture containing the nitrosated product, and a carbonyl compound of the formula <IMAGE> in which A denotes an aromatic hydrocarbon group or an aromatic heterocyclic group, which groups can contain a substituent, and B denotes a hydrogen atom, an alkyl group, an aryl group or an aromatic heterocyclic group, which groups can contain a substituent, is then added to the mixture containing the N,N-disubstituted hydrazine, as a result of which condensation of the N,N-disubstituted hydrazine with the carbonyl compound is carried out.
申请公布号 DE3331259(A1) 申请公布日期 1984.03.01
申请号 DE19833331259 申请日期 1983.08.30
申请人 CANON K.K. 发明人 ARITA,TETSUO;MABUCHI,MINORU;UMEHARA,SHOJI;SAKAI,KIYOSHI
分类号 C07C249/16;C07D209/86;C09B26/02;G03G5/06;(IPC1-7):C07C109/16;C07C109/12 主分类号 C07C249/16
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