发明名称 PROCESS FOR OBTAINING A TYPE A CRYSTALLINE SILICOALUMINATE WITH HIGH WATER REGAIN, AND ESPECIALLY OF TYPE 4A, AND PRODUCT SO OBTAINED
摘要 1. A process for producing a zeolite of type A with a high water absorption capacity, with an SiO2 / AI2 O3 molar ratio higher than 1.85 and advantageously at least equal to 2, characterized in that : (a) a mixture of solutions of sodium aluminate and silicate is made from a solution of aluminate which is advantageously cooled at from -10 to +10 C, and a solution of silicate, at a temperature such that the temperature of the resulting medium is substantially lower than the ambient temperature, with sufficient agitation being maintained to permit the formation of a homogenous solution having the appearance of a gel and with the molar ratio in the reaction medium being maintained at a value which is at least equal to 1.85 ; (b) the temperature of the reaction medium is raised to a value in the range of from 60 to 100 C ; (c) the medium is maintained at that temperature for a sufficient period of time of from 0.2 to 5 h, so as to cause crystallisation and redispersion of the silicoaluminate in the form of suspension of crystals in the liquid phase, and (d) the resulting crystals are separated and dried.
申请公布号 DE3160890(D1) 申请公布日期 1983.10.27
申请号 DE19813160890 申请日期 1981.01.08
申请人 RHONE-POULENC CHIMIE DE BASE 发明人 LATOURRETTE, BERTRAND
分类号 C01B39/16;B01J;C01B;C01B39/02;C01F7/02;(IPC1-7):C01B33/28 主分类号 C01B39/16
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