发明名称 |
Process for the isolation of 1-naphthylamine-4,8-disulphonic acid |
摘要 |
Process for the isolation of 1-naphthylamine-4,8-disulphonic acid from sulphonation mixtures containing it according to which process the sulphonation mixture is introduced into preheated water in such a manner that, at the start of crystallization, a temperature of at least 100 DEG C. is reached and the 1-naphthylamine-4,8-disulphonic acid is separated from the mother liquor at a temperature not higher than 70 DEG C. The process is applied particularly advantageously for the isolation of 1-naphthylamine-4,8-disulphonic acid from sulphonation mixtures which have been obtained by introducing in turns alkali metal sulphate, 1-naphthylamine-8-sulphonic acid and SO3 into sulphuric acid which has been introduced initially, a total of 1.5 to 3 mols of SO3 and 0.6 to 1.5 mols of alkali metal sulphate being employed per mol of 1-naphthylamine-8-sulphonic acid.
|
申请公布号 |
US4407762(A) |
申请公布日期 |
1983.10.04 |
申请号 |
US19820410746 |
申请日期 |
1982.08.23 |
申请人 |
BAYER AKTIENGESELLSCHAFT |
发明人 |
BLANK, HEINZ U.;BEHRE, HORST;LINDEN, HANS W.;MENTZEL, WERNER |
分类号 |
C07C309/47;C07C67/00;C07C301/00;C07C303/44;(IPC1-7):C07C143/60 |
主分类号 |
C07C309/47 |
代理机构 |
|
代理人 |
|
主权项 |
|
地址 |
|