发明名称 Process for conditioning reducible cyclic organic compounds
摘要 A process for purifying cyclic organic compounds such as phenol, aniline and nitro benzene which are readily reducible by catalytic hydrogenation and stable under the conditions of the process, comprises mixing the organic compound with ethylenediamine-tetraacetic acid or an alkali metal or ammonium salt thereof preferably the trisodium salt as conditioning agent preferably in an amount of 0.015-0.1% (calculated as the trisodium salt of the ethylenediaminetetraacetic acid), by weight of the cyclic organic compound, heating the mixture at a temperature of at least 80 DEG C. and preferably at least 150 DEG C. for at least one hour and distilling off the compound from the mixture. Where phenol or aniline is being purified they are mixed with caustic alkali as well as the conditioning agent which is employed in an amount about equal to the weight of the conditioning agent. Examples are given of the purification of phenol, aniline and nitrobenzene.
申请公布号 US3187050(A) 申请公布日期 1965.06.01
申请号 US19610093868 申请日期 1961.03.07
申请人 ALLIED CHEMICAL CORPORATION 发明人 DUGGAN RAYMOND J.;WINSTROM LEON O.
分类号 B01J31/02;C07B61/00;C07C37/74;C07C201/16;C07C209/36 主分类号 B01J31/02
代理机构 代理人
主权项
地址