发明名称 Method for the production of blocked isocyanates
摘要 Blocked isocyanates of the general formula <IMAGE> are obtained by converting terephthalic dialdoxime, isophthalic dialdoxime or an aliphatic, cycloaliphatic or aromatic ketoxime or an aromatic aldoxime of the general formula <IMAGE> in the presence of 10-100 Mol % sodium, potassium or calcium hydroxide, with the sodium, potassium or calcium salt of a bis-N-chloramide of the general formula Cl-NH-CO-R-CO-NH-Cl in water or a mixture of water and an aprotic solvent. Preferred first components include terephthalic dialdoxime, benzaldehyde-, cyclohexanone-, acetone- and acetophenoneoxime. Preferred aprotic solvents include dimethyl acetamide, dimethylformamide, sulfolan and tetramethylurea.
申请公布号 US4393238(A) 申请公布日期 1983.07.12
申请号 US19810265321 申请日期 1981.05.18
申请人 AKZO NV 发明人 ZENGEL, HANS-GEORG;BERGFELD, MANFRED
分类号 C07C271/60;B01J23/02;B01J23/04;C07B61/00;C08G18/70;(IPC1-7):C07C131/00 主分类号 C07C271/60
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